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Extra info for Amino Acids in Animal Nutrition
C. and Toldra, F. (1991) Deproteinization for HPLC amino acid analysis in fresh pork muscle and dry-cured ham. Journal of Agricultural and Food Chemistry 39, 1792–1795. D. and Martelli, A. (1998) Ion-pair HPLC determination of biogenic amines and precursor amino acids. Application of a method based on simultaneous use of heptanesulfonate and octylamine to some foods. Chromatographia 48, 763–769. , Kuehn, R. and Moenschwitzer, U. (1994) Analysis of free amino-acids in green coffee beans. I. Determination of amino-acids after precolumn derivatization using 9-fluorenylmethylchloroformate.
2001) tested a taurine assay in pet food after acid hydrolysis (6 M HCl, 110°C, 16 h) and precolumn derivatization with dansyl chloride in a collaborative trial. 3% were achieved, and the procedure was adopted as the official method by AOAC International. Porter et al. (1988), Amiss et al. (1990), Sakai and Nagasawa (1992) and Messing and Sturmann (1993) described the determination of taurine in feline and other blood and plasma by HPLC separation following precolumn derivatization with different reagents.
Landry and Delhaye (1994b), who also participated, presented the view, as mentioned above, that 5methyltryptophan must be present during hydrolysis with barium hydroxide and that by using their special autoclaving conditions about 15% higher tryptophan concentrations are obtained than with other techniques. The second collaborative trial showed, however, that irrespective of the hydrolysis technique the use of this internal standard generated analytical values in all laboratories that were a significant 13–20% higher than with ␣methyltryptophan.
Amino Acids in Animal Nutrition by D_Mello